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LI

u/liv_nkemelu

Contributes reviews on supplier material. Based in Kaunas.

member · joined 12 Mar 2025

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Comments — page 4 of 4

comment on genuine question about bacteriostatic water that I am slightly embarrassed to ask in c/reconstitution · 1 points · 1 year ago

swirl, do not shake, or you are courting oxidation

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comment on genuine question about bacteriostatic water that I am slightly embarrassed to ask in c/reconstitution · 19 points · 1 year ago

The single most useful thing I did was write the concentration on the vial. Stopped all the confusion after that.

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comment on tried PBS for 8 weeks. here is what happened. in c/glp1aus · 6 points · 1 year ago

Slight fix: the number was 99.0, not 98.9.

Disagree on that part. 94.2% and 95.1% on the same vial is normal.

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comment on Spain: batch, and what it actually costs here in c/coa · 88 points · 1 year ago

The chromatogram trace is where the real information lives. The summary number is just a headline.

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comment on is it normal to get constipation at week 29 in c/reconstitution · 8 points · 1 year ago

Yeah, showing the arithmetic is the fastest way for someone to spot the error.

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comment on help me understand units, I have read the wiki twice in c/reconstitution · 22 points · 1 year ago

more water means more units for the same dose, which means finer resolution

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comment on the compounding question that gets asked weekly, answered properly in c/glp1aus · 57 points · 1 year ago

PBS listings change the cost completely

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comment on area percent — my 20-week log, condensed into one table in c/coa · 56 points · 1 year ago

Yeah, 96.8% area is not the problem, the missing impurity breakdown is the problem.

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comment on small win: shortage stopped being a problem at week 71 in c/glp1aus · 17 points · 2 years ago

Strongly agree. AU and NZ differ.

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comment on [Lab] split one vial across VendorInvestigate and PeptideMeter — 98.0% and 97.9% in c/coa · 164 points · 2 years ago

Disagree. What you are describing is consistent with certificate of analysis, not with what you concluded.

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comment on [Discussion] purity is doing more work than we give it credit for in c/coa · 67 points · 2 years ago

axis labels included, always

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comment on [Discussion] purity is doing more work than we give it credit for in c/coa · -24 points · 2 years ago

Metadata check caught a COA that was created in a browser four months after the analysis date. Not evidence of fraud, but worth flagging to QSC.

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comment on [Discussion] purity is doing more work than we give it credit for in c/coa · 267 points · 2 years ago

The chromatogram trace is where the real information lives. The summary number is just a headline.

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comment on dead space — 12 things I got wrong before I got it right in c/reconstitution · 6 points · 2 years ago

i am begging people to write down the concentration

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comment on dead space — 12 things I got wrong before I got it right in c/reconstitution · 75 points · 2 years ago

Dead space ate 13 units on a low-volume draw. Tiny impact at 1.0mg, massive impact at 0.5mg.

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comment on dead space — 12 things I got wrong before I got it right in c/reconstitution · 19 points · 2 years ago

more water means more units for the same dose, which means finer resolution

Disagree on that part. 96.8% and 96.2% on the same vial is normal.

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comment on help me understand batch, I have read the wiki twice in c/coa · 116 points · 2 years ago

Yeah, 96.8% area is not the problem, the missing impurity breakdown is the problem.

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comment on [Discussion] can we stop arguing about units until somebody posts a number in c/reconstitution · 31 points · 2 years ago

This is correct. 1mL versus 5mL is the common mistake.

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