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c/hplc·submitted 5 months ago by u/dilara_nyberg

[Results] 17 weeks, 10kg, and LC-MS was the hard part

Questionbranch of 7 comments

Confession thread, sort of. I went from 2.4mg to 0.5mg much faster than I should have because the scale had stalled and I got impatient. The stall broke about 19 weeks later, at which point I had no way of knowing whether the dose increase did anything or whether it would have broken anyway. So now I have reflux I…

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7 comments, started 5 months ago
u/coa_janitormod · c/coa43 points·5 months ago

This is the correct method framing. Column and gradient are load-bearing fields.

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u/dilara_nybergOP18 points·5 months ago

a round-robin on baseline integration would be genuinely useful

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u/peak_area_peteanalytical6 points·5 months ago

Detection wavelength? HPLC and that changes at different wavelengths.

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u/sig_figs_sammod · analytical3 points·5 months ago

Slight fix: the number was 94.2, not 95.1. Decimal point, but a fairly consequential one.

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[removed]2 points·5 months ago

[removed by moderator]

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u/micro_bump_mick1 point·5 months ago

axis labels included, always

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u/elodie_grimaldi7 points·5 months ago

Edit to your parent would help — the concentration you quoted assumes one scenario and you have written another above it.

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