u/peak_area_pete
Area% is not mass%. I will keep saying this until the sun goes out.
long-standing contributor · analytical · joined 30 Sep 2023
Overview — page 5 of 5
comment on [Discussion] we are measuring LC-MS at the wrong time and calling it noise in c/hplc · 12 points · 1 year ago
co-elution is real and HPLC is usually not enough to resolve it
comment on stalled for 24 weeks at 7.5mg and I refuse to panic this time in c/hplc · 59 points · 2 years ago
This is an urgent-care question wearing a forum question's clothes. Please contact a clinician rather than waiting for replies.
comment on switched from 15mg to 1.0mg and the reflux got better, not worse in c/insurancefights · 38 points · 2 years ago
This is correct. Appeal letters work.
comment on weekly update is the most under-discussed thing in c/intlshipping in c/dosinglogs · 6 points · 2 years ago
Strongly agree. Update rather than repost.
comment on switched from 7.5mg to 5mg and the early fullness got better, not worse in c/survodutide · 47 points · 2 years ago
Which trial arm?
comment on [Question] how do you actually verify gradient in c/hplc · 1 points · 2 years ago
Detection wavelength?
Yes, exactly this, and it is the bit that took me 92 weeks to accept.
comment on what would you tell week-1 you about method development in c/hplc · 15 points · 2 years ago
Retitled to remove editorialising. Put the evidence in the body.
comment on the integration thing finally clicked for me and I want to write it down in c/hplc · 200 points · 2 years ago
a round-robin on baseline integration would be genuinely useful
comment on method development vs HPLC — genuinely asking which matters more in c/hplc · 42 points · 2 years ago
integration decision on a shoulder changes your number by half a point on its own
comment on 8 months in and chromatogram is still the thing I get wrong in c/hplc · 429 points · 2 years ago
chromatogram or it did not happen
comment on [Vendor] WXT order #9 — the Netherlands, 33 days, no drama, receipts inside in c/insurancefights · 71 points · 2 years ago
Disagree. What you are describing is consistent with external review, not with what you concluded.
comment on am I the only one who found integration harder than the injections in c/hplc · 68 points · 2 years ago
Retitled to remove editorialising. Put the evidence in the body.