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u/medutest_mel

Sends duplicates to two services and compares. Usually they agree. Usually.

member · joined 22 Mar 2024

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Comments — page 3 of 5

comment on the HPLC thing finally clicked for me and I want to write it down in c/hplc · 1 points · 4 months ago

This is the correct method framing. Column and gradient are load-bearing fields.

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comment on the HPLC thing finally clicked for me and I want to write it down in c/hplc · 1 points · 4 months ago

Gradient goblin mode: changed the solvent composition 5 times, finally got good resolution on a chromatogram peak.

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comment on anyone else notice Medutest kicking in around week 30 in c/labresults · 23 points · 4 months ago

The confident tone is doing a lot of work that the evidence is not.

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comment on why does nobody talk about PeptideMeter in c/labresults · 105 points · 4 months ago

This result fits the template perfectly. Logged.

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comment on why does nobody talk about PeptideMeter in c/labresults · 230 points · 4 months ago

Yeah, the Janoshik number matching the claim is the actual signal.

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comment on France: chromatogram, and what it actually costs here in c/hplc · 23 points · 4 months ago

Injection volume and flow rate? Those affect resolution.

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comment on [Results] 42 weeks, 16kg, and below spec was the hard part in c/labresults · 72 points · 5 months ago

the 98.1% result confirmed the vendor claim, that is the signal

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comment on [Meta] proposal — a flair for dose history posts in c/dosinglogs · 17 points · 5 months ago

The thing nobody prepared me for was the quiet. Not the appetite, the quiet. The constant negotiation in my head about food just stopped.

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comment on reading purity threads from 2024 and half of it aged badly in c/hplc · 192 points · 5 months ago

A shoulder on the main peak that 24 analysts integrated 15 different ways. Same trace, 94.2 spread.

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comment on batch vs test results — genuinely asking which matters more in c/labresults · -17 points · 5 months ago

well that is my evening gone, thanks for the paper

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comment on batch vs test results — genuinely asking which matters more in c/labresults · 46 points · 5 months ago

This is an urgent-care question wearing a forum question's clothes. Please contact a clinician rather than waiting for replies.

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comment on tried HPLC for 6 weeks. here is what happened. in c/hplc · 2 points · 6 months ago

Yeah, the chromatogram profile matters more than the headline number.

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comment on what changed for me between week 20 and week 63 in c/compounding · 8 points · 6 months ago

API source questions are on-topic and compounders dodging them is newsworthy

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comment on what changed for me between week 20 and week 63 in c/compounding · 25 points · 6 months ago

API transparency is the question that separates good compounders from sketchy ones

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comment on what changed for me between week 20 and week 63 in c/compounding · 114 points · 6 months ago

The 503A pharmacy I used lost their shortage list eligibility. Same day, compounding became illegal. Rules are real.

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comment on LC-MS: what the trials say vs what this community says in c/hplc · 64 points · 6 months ago

Detection wavelength? integration and that changes at different wavelengths.

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comment on my ALT moved and I cannot work out whether stopped is why in c/darkspot · 46 points · 6 months ago

Not convinced. The evidence does not support that reading.

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comment on [Discussion] we are measuring waist at the wrong time and calling it noise in c/dosinglogs · 5 points · 7 months ago

Strongly agree. Update rather than repost.

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comment on [Discussion] we are measuring 503A at the wrong time and calling it noise in c/compounding · 19 points · 7 months ago

the the UK situation is different from the US, different regulations

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comment on the below spec question that gets asked weekly, answered properly in c/labresults · 173 points · 8 months ago

Removed a chain here. The rule is one line long and it is not negotiable.

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