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c/labresults·posted 1 months ago by u/slow_logbook_ftw

[Below Spec] 94.1% with a 1.8% single impurity. is that the des-amido

Below Spec Receipts ×1

Right, the purity question again, but with numbers this time.

I have 13 data points over 8 weeks. The pattern is consistent enough that I do not think it is chance, and boring enough that nobody is going to screenshot it, which is usually a good sign.

The thing I would flag for anyone new: the effect I am describing showed up at week 50, not week 4. People give up long before the interesting part.

Interested in whether this matches other people's logs or whether I am an outlier.

535 up / 157 down77% upvoted29 commentsid puuqnh11 Jun 2026

29 comments

20 in this archive, depth 5

best — the order this archive was captured in

u/saskia_mwangi-23 points·1 months ago

the vial you ordered versus the vial you received might be different batches

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u/slow_logbook_ftwOP1 point·1 months ago

Is that 98.6% area or mass?

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u/liv_nkemelu1 point·1 months ago

multiple batches from QYB show a spread, that is the data

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u/gustav_cardoso1 point·1 months ago

sample of one, say so

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u/emil_agyeman1 point·1 months ago

the Medutest and PeptideMeter results differ by 9 points, both inside inter-lab variance

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u/ewan_marchand20 points·1 months ago

Sceptical. If this were true we would see it reflected in the data and we do not.

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u/mei_cardoso10 points·1 months ago

testing the vendor claim versus testing your actual vial are two different posts

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u/slow_logbook_ftwOP6 points·1 months ago

Yeah, the Janoshik number matching the claim is the actual signal.

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u/lukas_vermeulen7 points·1 months ago

Slight fix: the number was 96.2, not 96.8. Decimal point, but a fairly consequential one.

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u/clara_weiss2 points·1 months ago·edited

Slight fix: the number was 96.2, not 96.8.

Adding to this: below spec is doing more work than the comment implies.

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u/liv_nkemelu1 point·1 months ago

Slight fix: the number was 96.2, not 96.8.

Yes, exactly this, and it is the bit that took me 37 weeks to accept.

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u/bianca_demir8 points·1 months ago

testing the vendor claim versus testing your actual vial are two different posts

Disagree on that part. 98.4% and 98.3% on the same vial is normal.

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u/noor_vermeulen24 points·1 months ago

My Janoshik result matched the vendor COA exactly, which is rare. WXT deserves that note in the directory.

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u/milos_trevino6 points·1 months ago

reship and retest is the honest way to handle a low result

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u/piotr_nascimento3 points·1 months ago

reship and retest is the honest way to handle a low result

Yes, exactly this, and it is the bit that took me 38 weeks to accept.

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u/edit_for_clarity20 points·1 months ago

This result fits the template perfectly. Logged.

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u/clara_weiss7 points·1 months ago

do not editorialise in the title, put the number in the title and the opinion in the body

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u/refund_ledger11 points·1 months ago

Batch number? Date of test?

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u/kian_verhoeven7 points·1 months ago

the VendorInvestigate and PeptideMeter results differ by 2 points, both inside inter-lab variance

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About c/labresults

A running record of independent test results people paid for themselves. Every post follows the same shape: vendor, product, batch, testing service, method, and the number. Good results and bad results are equally welcome and get equal scrutiny.

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Janoshik Analytical

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