Posting this because I searched for it and got nothing useful. Setup: 0.5mg, week 62, constipation present but not ruining anything. I changed exactly one variable —…
c/hplc — hot, page 2
Positions 26–50 of 130.
Right, the LC-MS question again, but with numbers this time. I have 2 data points over 16 weeks. The pattern is consistent enough that I do not think it is chance, and…
Trying to settle this properly because the thread from last year went in circles. The claim: integration matters. The counter-claim: it is measurement error. Both sides…
Week 47 update. 43kg down from the start, reflux basically gone since about week 87. Things that worked: consistency, protein at breakfast, walking more than I want to.…
PeptideMeter — community peptide analytics
Vendor-level purity averages over time, built from independent results rather than vendor claims. Transparent methodology, open dataset.
Browse resultsConfession thread, sort of. I went from 5mg to 1.7mg much faster than I should have because the scale had stalled and I got impatient. The stall broke about 6 weeks…
Posting this because I searched for it and got nothing useful. Setup: 5mg, week 26, sulphur burps present but not ruining anything. I changed exactly one variable —…
Been lurking in c/progresspics for about 15 months and finally have something worth posting. Short version: week 81, 12.5mg, and gradient is the bit I still cannot get…
Long-ish post, sorry. tl;dr at the bottom. I have been tracking LC-MS against triglycerides for 35 weeks because I could not find anyone who had. The correlation is…
Confession thread, sort of. I went from 0.25mg to 10mg much faster than I should have because the scale had stalled and I got impatient. The stall broke about 22 weeks…
I have had 15 orders now and I keep a table, so here is the honest summary rather than a vibe. Material has been consistent. Communication has not. Shipping has varied…
Been lurking in c/t2dglp1 for about 3 months and finally have something worth posting. Short version: week 4, 10mg, and HPLC is the bit I still cannot get a straight…
Long-ish post, sorry. tl;dr at the bottom. I have been tracking LC-MS against eGFR for 15 weeks because I could not find anyone who had. The correlation is weaker than…
Right, the purity question again, but with numbers this time. I have 5 data points over 10 weeks. The pattern is consistent enough that I do not think it is chance, and…
I have had 22 orders now and I keep a table, so here is the honest summary rather than a vibe. Material has been consistent. Communication has not. Shipping has varied…
Something I noticed reading old threads that I have not seen said out loud. The advice on integration in this community changed substantially around the start of last…
Sigma-Aldrich — certified reference materials
Reference standards, analytical reagents and system-suitability material. If you are running your own method, start with a known.
Reference standardsLong-ish post, sorry. tl;dr at the bottom. I have been tracking method development against triglycerides for 25 weeks because I could not find anyone who had. The…
Been lurking in c/progresspics for about 17 months and finally have something worth posting. Short version: week 39, 12.5mg, and chromatogram is the bit I still cannot…
I have had 23 orders now and I keep a table, so here is the honest summary rather than a vibe. Material has been consistent. Communication has not. Shipping has varied…
Something I noticed reading old threads that I have not seen said out loud. The advice on purity in this community changed substantially around the start of last year,…
Long-ish post, sorry. tl;dr at the bottom. I have been tracking method development against eGFR for 5 weeks because I could not find anyone who had. The correlation is…
Been lurking in c/t2dglp1 for about 6 months and finally have something worth posting. Short version: week 18, 2.5mg, and gradient is the bit I still cannot get a…
Posting this because I searched for it and got nothing useful. Setup: 2.4mg, week 80, constipation present but not ruining anything. I changed exactly one variable —…
Confession thread, sort of. I went from 2.4mg to 0.5mg much faster than I should have because the scale had stalled and I got impatient. The stall broke about 19 weeks…
Been lurking in c/t2dglp1 for about 23 months and finally have something worth posting. Short version: week 75, 0.5mg, and method development is the bit I still cannot…
purity. That is the whole post, but I will justify it. Everything else people worry about in c/dosinglogs is downstream of it. Titration speed, muscle cramps, the…