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c/coldchain·posted 2 years ago by u/priya_weiss

does lyophilised actually matter or is it forum lore at this point

Explainer Receipts ×4 Well Actually ×2 Cold Box ×3

does lyophilised actually matter or is it forum lore at this point, and I want the answer with the reasoning attached rather than just the conclusion.

Gel packs are designed for a duty cycle. A liquid pack at the end of a longer-than-expected transit is a pack behaving as specified, not evidence of an excursion in the vial.

Lyophilisation removes the water that drives most degradation pathways. That is why the dry cake is comparatively robust and the reconstituted solution is not.

Once in solution, the relevant risks are hydrolysis, aggregation and, for some sequences, oxidation. Refrigeration slows all three; freezing a solution introduces a separate risk at the ice interface.

Please do not ask me what dose you should be on. I genuinely do not know and neither does anyone else here.

3,312 up / 649 down84% upvoted48 commentsid ua7zt024 Mar 2024

48 comments

27 in this archive, depth 4

best — the order this archive was captured in

u/plain_titration_2024393 points·2 years ago·edited

A transit temperature logger records a distribution, and time above a threshold matters as much as peak temperature. That is the argument for logging rather than guessing.

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u/aleksi_eriksen308 points·2 years ago

Ordered from the warehouse in the Netherlands instead of origin and the transit went from a fortnight to 13 days. Entirely different proposition in August.

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u/priya_weissOP126 points·2 years ago

Wrote the reconstitution date on the vial for the first time last year. Have never once since wondered how old a solution is.

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u/osman_eriksen186 points·2 years ago

Cosigning the regional stock point. Ordering from a warehouse in the UK took the whole question off my table.

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u/osman_brandt46 points·2 years ago

Cosigning the regional stock point.

osman_eriksen is right that the pack failing is not the material failing. Two separate claims.

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u/priya_weissOP84 points·2 years ago

a warm gel pack tells you the pack failed, not that the material did

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u/ferran_laurent-28 points·2 years ago

How many days in transit, and which month?

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u/curious_panel_only122 points·2 years ago

Regional stock changes the question rather than answering it: shorter lanes mean less exposure and fewer variables, which is why the warehouse question is worth asking before ordering in summer.

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u/ice_pack_auditcold chain33 points·2 years ago

Seasonality, which the source-page lane tables show clearly once you look for it.

The same origin, destination and carrier can differ by several days between February and August, and the temperature exposure differs by much more than the transit time suggests. A lane that is uneventful in winter is the same lane that generates the summer threads.

Two practical consequences. First, compare like months when you compare lanes. Second, ask which lines a supplier holds in regional stock — a shorter leg in July is worth more than any amount of packaging.

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u/andres_restrepo80 points·2 years ago

Right, and asking what the stability statement was written against is one line of email that reframes everything.

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u/osman_eriksen63 points·2 years ago

a logger costs less than a vial and answers the question permanently

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u/runa_wikstrom33 points·2 years ago

This. A liquid gel pack on arrival tells you about the pack’s duty cycle, not about the vial.

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u/low_appetite_lisa48 points·2 years ago

regional stock removes most of this problem entirely

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u/preservative_free_p96 points·2 years ago

A stability statement is only meaningful with its conditions attached: temperature, duration, light exposure, and whether it covers powder or solution. Ask which.

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u/bruno_dumitru114 points·2 years ago

lyophilised powder is far more forgiving than the panic threads suggest

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u/tidy_vialdrawer_watch2841 points·2 years ago

the door shelf is the worst place in the fridge

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u/sten_palacios36 points·2 years ago

a summer lane and a winter lane are different lanes

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u/ireland_drugs_pay60 points·2 years ago

Asked FGP which lines they hold regionally and got a straight list back. That answered my summer ordering question completely.

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u/hplc_hobbyistruns their own column21 points·2 years ago

transit temperature is a distribution, not a number

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u/split_dose_sceptic11 points·2 years ago

Yes — reconstitution date on the vial. It is the number you will want and cannot reconstruct.

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u/priya_weissOP12 points·2 years ago

Is this a line they hold in regional stock or is it shipping from origin?

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u/coldchain_karencold chain3 points·2 years ago

light matters more than people think for some of these

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u/ines_lindqvist18 points·2 years ago

ask which lines are held in regional stock before you order in July

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Temperature and stability in the real world: what an excursion actually costs you, why lyophilised powder is far more forgiving than reconstituted solution, how to read a logger CSV, and how to photograph a failed shipment so the conversation with the vendor is short.

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